By Claude S. Hudso (ed.), Sidney M. Canto (ed.)
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Drew, E. H. Goodyear and W. N. Hrtworth, J . Chem. , 1237 (1929). (52) J. Pryde, E. L. Hirst and R. W. Humphreys, J . Chem. , 127, 348 (1925). This Page Intentionally Left Blank THE SYNTHESIS OF OLIGOSACCHARIDES BY W. L. EVANS, D. D. REYNOLDSAND E. A. TALLEY The Ohio State University, Eastman Kodak Company, Eastern Regional Research Columbus, Ohio Rochester, New York Laboratory, U. S. Department of Agriculture, Philadelphia, Pennsylvanaa CONTENTS I. Introduction . . . . . . . . . . . .
Bourquelot and M. Bridel, J . pharm. , 6, 13,56, 193 (1912). (30) E. Bourquelot, J . pharm. , 10, 361,393 (1914). Bourquelot and M. Bridel, Compl. , 168, 253 (1919). THE SYNTHESIS OF OLIGOSACCEARIDES 37 beta linkages, and another enzyme, a-D-glucopyranosidase, the syntheses of alpha linkages. Studies on the reactions have indicateda2 that the syntheses of cellobiose and gentiobiose follow the law of mass-action if allowance be made for the displacement of the equilibrium between a-D-glucose and p-D-glucose either by solvent or by concentration of the solution, and also for the concentration of the actual activated form of D-glucose.
S8, 1178 (1925). H. Vogel and H. Debowska-Kurnicka, Helv. Chim. Acta, 11, 910 (1928). A. M. Gakhokidze, J . Gen. Chem. ( U . S . S . ), 11, 117 (1941). A. M. Gakhokidze, J . Gen. Chem. ( U . S. S . ), 16, 1923 (1946). A. M. Gakhokidze, Trudy Tbilis Uchitel. Znst. S. 8. R . ) ) , 2, 146 (1941). (53) W. J. Hickinbottom, J . Chem. ,1676 (1929). (53a) P. Brigl, 2. physiol. , 116, 1 (1921). (54) In the experimental part of the paper,60 silver carbonate was mentioned as the reagent but the amounts used agree for silver acetate which also is given as the reagent in the introduction of the paper.